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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface / Supramolecular Ordering, Electronic Properties and Reactivity / Florian Buchner / Buch / Springer Theses / Englisch - Buchner, Florian
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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface / Supramolecular Ordering, Electronic Properties and Reactivity / Florian Buchner / Buch / Springer Theses / Englisch - gebunden oder broschiert

2010, ISBN: 9783642148392

[ED: Gebunden], [PU: Springer Berlin], The functionalization of surfaces on the nanoscale is one of the most fascinating and at the same time challenging topics in science. It is the key … Mehr…

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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface Supramolecular Ordering, Electronic Properties and Reactivity - gebunden oder broschiert

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Gebundene Ausgabe Chemie / Analytisch, Energietechnik, Festkörperphysik, Chemie, Massenspektrometrie - Spektrometrie , Spektroskopie, Chemie (physikalisch), Physik / Chemie, Physikalisc… Mehr…

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Stm Investigation of Molecular Architectures of Porphyrinoids on a Ag111 Surface Supramolecular Ordering, Electronic Properties and Reactivity Springer Theses - gebunden oder broschiert

2011

ISBN: 9783642148392

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Stm Investigation of Molecular Architectures of Porphyrinoids on a Ag111 Surface Supramolecular Ordering, Electronic Properties and Reactivity Springer Theses - gebunden oder broschiert

2011, ISBN: 9783642148392

Hardcover, PLEASE NOTE, WE DO NOT SHIP TO DENMARK. New Book from multilingual publisher. Shipped from UK within 4 to 14 days. Please check language within the description., [PU: Springer]

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Stm Investigation of Molecular Architectures of Porphyrinoids on a Ag111 Surface Supramolecular Ordering, Electronic Properties and Reactivity Springer Theses - gebunden oder broschiert

2011, ISBN: 9783642148392

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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface: Supramolecular Ordering, Electronic Properties and Reactivity (Springer Theses)

The self-assembly of large organic molecules has become a vividly explored and interdisciplinary field in science. One major goal is the tailored fabrication of highly ordered, molecular networks, which are stabilized on a metal surface. Metalloporphyrins receive particular attention, because their distinct intrinsic functionalities make them promising candidates for applications in chemical sensors, solar cells, and for tailored catalytic processes. Based on scanning tunneling microscopy investigations, several novel and fundamental contributions are presented, which has led to a new level of understanding. Highlights are the results with respect to intramolecular conformation and supramolecular ordering, electronic interactions with the substrate, surface confined synthesis such as in-situ metallation reactions, and ligand effects.The number of publications this work has led to emphasises its quality and significance.

Detailangaben zum Buch - STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface: Supramolecular Ordering, Electronic Properties and Reactivity (Springer Theses)


EAN (ISBN-13): 9783642148392
ISBN (ISBN-10): 3642148395
Gebundene Ausgabe
Erscheinungsjahr: 2010
Herausgeber: Springer

Buch in der Datenbank seit 2014-02-19T16:42:49+01:00 (Vienna)
Detailseite zuletzt geändert am 2022-04-06T20:17:49+02:00 (Vienna)
ISBN/EAN: 9783642148392

ISBN - alternative Schreibweisen:
3-642-14839-5, 978-3-642-14839-2


Daten vom Verlag:

Autor/in: Florian Buchner
Titel: Springer Theses; STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface - Supramolecular Ordering, Electronic Properties and Reactivity
Verlag: Springer; Springer Berlin
164 Seiten
Erscheinungsjahr: 2010-11-11
Berlin; Heidelberg; DE
Gedruckt / Hergestellt in Niederlande.
Gewicht: 0,494 kg
Sprache: Englisch
139,09 € (DE)
142,99 € (AT)
153,50 CHF (CH)
POD
XXVII, 164 p.

BB; Book; Hardcover, Softcover / Chemie/Physikalische Chemie; Physikalische Chemie; Verstehen; Chemie; Porphyrinoids; STEM; STM; Scanning Tunneling Microscopy; Scanning Tunneling Spectroscopy; Self-assembly; Supra; Supramolecular Chemistry; Surface Chemistry; electronics; B; Physical Chemistry; Analytical Chemistry; Solid State Physics; Surface and Interface Science, Thin Films; Energy Systems; Physical Chemistry; Analytical Chemistry; Condensed Matter Physics; Surface and Interface and Thin Film; Electrical Power Engineering; Mechanical Power Engineering; Chemistry and Materials Science; Analytische Chemie; Physik der kondensierten Materie (Flüssigkeits- und Festkörperphysik); Physik der kondensierten Materie (Flüssigkeits- und Festkörperphysik); Elektrotechnik; Energietechnik, Elektrotechnik und Energiemaschinenbau; BC; EA

1 Introduction ...................................................................................................... 1 2 Fundamentals .................................................................................................... 5 2.1 Principle of the STM ............................................................................................ 5 2.2 Origin of the Tunneling Current ........................................................................... 7 2.3 Scanning Tunneling Spectroscopy ...................................................................... 10 2.4 Contrast Mechanism of Molecular Adsorbates ................................................... 13 2.5 Temperature Programmed Desorption ................................................................ 16 2.6 Low Energy Electron Diffraction ....................................................................... 18 3 Experimental Setup ........................................................................................ 21 3.1 UHV System ...................................................................................................... 21 3.2 Scanning Tunneling Microscope ........................................................................ 23 3.3 Control Electronics and Vibration Isolation ........................................................ 26 3.4 Ag(111) ............................................................................................................. 28 3.5 Porphyrinoids..................................................................................................... 30 3.6 Preparation of thin Porphyrinoid Layers ............................................................. 33 3.7 Vapor-deposition of Cobalt and Iron .................................................................. 34 4 Results ............................................................................................................. 39 4.1 Self-Assembly and Individual Appearance of Tetraphenylporphyrins on Ag(111) ............................................................................................................. 41 4.1.1 Epitaxial growth ........................................................................................... 43 4.1.2 Appearance and Intramolecular Conformation .............................................. 48 4.1.3 Ordering Aspects.......................................................................................... 50 4.2 Self-Assembly and Individual Appearance of Cobalt(II)-Tetrakisditertbutylphenylporphyrins on Ag(111) ......................................................................... 61 4.2.1 Polymorphism of CoTTBPP ......................................................................... 62 4.2.2 Polarity-Dependent Appearance ................................................................... 78 ii Table of Contents 4.3 Coordination of Iron and Cobalt Atoms by Tetraphenylporphyrin Monolayers on Ag(111) and Formation of Metal(II)-Tetraphenylporphyrin ......... 83 4.3.1 Coordination of Post-deposited Iron Atoms by Tetraphenylporphyrin Monolayers ................................................................................................... 85 4.3.2 Coordination of Pre-deposited Iron Atoms by Tetraphenylporphyrin Monolayers ................................................................................................... 90 4.3.3 Coordination of Post-deposited Cobalt Atoms by Tetraphenylporphyrin Monolayers ................................................................................................... 94 4.3.4 Discussion of the Metalation Reaction .......................................................... 99 4.4 Different Aspects of 2H-Tetrakisditertbutylphenylporphyrin on Ag(111) .. 103 4.4.1 Monolayer Preparation................................................................................ 104 4.4.2 Arrangement of 2HTTBPP ......................................................................... 107 4

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